Formation of Particles in Sol-Gel Process

Aqueous Sol-Gel Process for Protein Encapsulation

Porous silica materials made by low-temperature sol-gel process are promising host matrixes for encapsulation of biomolecules. To date, researchers have focused on sol-gel routes using alkoxides such as tetramethyl orthosilicate (TMOS) and tetraethyl orthosilicate (TEOS) for encapsulation of biomolecules. These routes lead to formation of alcohol as a byproduct that can have a detrimental effec...

Chemistry and Fundamentals of the Sol–Gel Process

Dimethylamine Controlled Sol-Gel Process to Grow ZnO Nanorods

ZnO nanorods were prepared using dimethylamine (DMA) controlled Sol-Gel process. Dimethylamine was added as an additive to control the sol-gel process for growing ZnO nanorods. DMA would exhibit stabilizing effect, promote dissolution of precursor and control the rate of sol-gel reactions because of its basic nature and significant miscibility. The Structural and microstructural properties of t...

Synthesis and Characterization of ZnO Nanoparticles Using Sol-gel Process

In the Present work structural, morphological and compositional properties of ZnO nanopowders synthesized using Zinc nitrate and NaOH using sol-gel process were reported. The synthesized nanopowders were further analyzed using X-Ray Diffraction (XRD), Scanning electron microscopy (SEM) and Fourier Transform Infrared (FTIR) spectroscopic characterizations. Crystalline size and Lattice strain det...

Optical sol-gel coatings : ellipsometry of film formation

2014 A method was developed to image an area of a drying, steady-state film during dip-coating using ellipsometry, thereby obtaining the film’s thickness and refractive index as a function of position. Measurements on TiO2 and SiO2 alcohol-based sols indicate that the film approaches a volume fraction 03A6 ~ 0.2 in the wet state and suggests that the film resists densifying further for kinetic ...